Humboldt State University ® Department of Chemistry

Robert A. Paselk Scientific Instrument Museum

Abbe Refractometer

Carl Zeiss/Jena

19201

Humboldt State College c. 1938

Usage/History: The Abbe refractometer provides a quick and easy means for determining refractive index and dispersion of liquids and solids. It is used in the examination of organic compounds (oils, solvents, etc.), solutions, food products, and serum protein concentration. The refractive index is measured by aligning the crosshairs in the telescope with the line of total reflection. This line is moved by rotating the prism assembly with the alidade. Reading at constant temperature is important, thus the prisms are enclosed in a water jacket which may be connected to a constant temperature bath.
Ernst Abbe published his Neue Apparate.... (1874)2 in which he discussed the theory and described instruments for the measurement of refractive index using prisms and by total reflection. It is here that he first describes the Abbé refractometer for determining the refractive index of fluids. This initial instrument includes Amici prisms and is essentially the same as a modern Abbé refractometer, though without temperature jacketing. An instrument very similar to that described by Abbe in 1874 was shown in catalogs beginning in 18933, shortly after the formation of the Instrument Department of the Carl Zeiss works in 1890.4 This style, with slight modifications5, continued to be seen in catalogs at least until 1910. A new design, apparently identical to the specimen in this collection, appears in a catalog of Zeiss instruments exhibited in Dresden in 1911.6 This instrument appears in catalogs at least as late as 1927.7 By 1934 this design had been modified by placing the mirror on a swinging arm attached to the prism axis and by adding a rack and pinion adjustment to the alidade.
Early descriptions of the features and use of the Abbe refractometer are provided below:
Description: The instrument stands 11.5" high in the closed, vertical position. The base is of cast iron with polished black enamel on the coved edge and the remainder in crinkle finish. There is a small tag affixed to the base with screws inscribed with the Carl Zeiss Jena "achromatic lens" logo, with Germany beneath it. The scale and readout arms are of steel. The scale is engraved on an inlaid German silver strip with scale divisions to the thousands place (nD 1,300-1,700), and numbered to the hundreds place. Readout is via a hairline engraved on a glass window affixed with screws to the readout arm beneath an adjustable magnifier. The refractometer telescope is heavy nickel-plated brass, with the Zeiss logo engraved on the front over the serial number: Nr. 15645. The Amici color compensating prism scale is black enameled with white filled engraved divisions (0-60-0) and adjusted with a knurled wheel. The prism holder is in flat black enameled brass with tubulatures for connecting to a circulating bath for temperature control. There is a screw-in brushed brass thermometer holder on the upper rear bath connection (shop made at Humboldt?). Miscellaneous hardware and screws are nickel-plated. Engraved: 5374 HSC.
The instrument is in its original light hardwood (maple?) case (8 1/4 x 6 3/4 x 14" h), with a black painted iron carry-handle and silver plated keyhole cover.
Research: A refractometer apparently identical with this specimen is illustrated in a catalog of Zeiss instruments exhibited in Dresden in 1911.6 This instrument appears in vendor catalogs at least as late as 1927.7A similar instrument, by Carl Zeiss, Jena, but with a gear drive for prism movement and the mirror mounted on the prism axis instead of the base, is illustrated in the Braun Corp. Catalog 34 (1934) as items 55630/1 on pg 654. A completely new & different model from Carl Zeiss is described in the Braun-Knecht-Heimann-Co. div of Van Waters & Rogers, Inc, Catalog No. 63 (©1961) on pg 885. HSU computer records indicate that this instrument was acquired in November of 1956, however, the HSC property number and its appearance in the HSC inventory book with other instruments acquired by Humboldt in the mid- to late 1930's indicate it was actually purchased c. 1938.
1 "No. 15645 was produced before February, 19., 1920 and delivered to Sussfield, Lorsch & Co. in New York on February 27 1920." Personal communication (1998), Dr. Wolfgang Wimmer, Archivar, Carl Zeiss Jena GMBH. However, see Research above.
2 Abbé, E. Neue Apparate zur Bestimmung des Brechungs - und Zerstreuungsvermögens fester und flüssiger Körper. Mauke's Verlag, Jena (1874) Taffel: Fig. 5-7.
3 Carl Zeiss Optical Works. Optical Measuring Instruments. Carl Zeiss Optical Works, Jena (1893) pp 9, 10.
4 Auerbach, Felix. The Zeiss Works and the Carl Zeiss Foundation in Jena. (English translation by R Kanthack) W. & G. Foyle, Ltd, London (1925).
5 Zeiss. Abbe's Refractometers. 3rd Edition (Mess. 172). Carl Zeiss, Jena (1907) pp 2 & 9.
6 Carl Zeiss Optical Works. Catalogue to the Collection of Optical Instruments Exhibited by the Carl Zeiss Optical Works Jena. Dresden International Hygiene Exhibition (1911) pg 13.
7 Cenco. Laboratory Apparatus for Chemical, Industrial, Metallurgical, Bacteriological, Board of Health, Clinical, Hospital and Commercial Testing Laboratories. Catalog C. Central Scientific Company, Chicago (1927) pg 592. The engraving in this catalog appears to be identical to the one used in 1911 in reference 10, above.

HSC (1935-1953)

 

HSTC (1921-34)

HSC 1936-53 Scientific Instruments

HSC (1954-1973)
© R. Paselk
Last modified 21 Appril 2008